Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose1

Arun K. Sarkar; Sushama M. Pawar; Khushi L. Matta

doi:10.1080/07328309108543906

Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose¹

Arun K. Sarkar
, Sushama M. Pawar
, Khushi L. Matta

Department of Chemical and Biological Engineering

Roswell Park Cancer Institute

Research output: Contribution to journal › Article › peer-review

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Abstract

Synthesis of three tetrasaccharides, namely, 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(l-*3)-0-(β-D-galactopyranosyl)- (1 ->4)-β-D-glucopyranose (7), 0-α-L-fucopyranosyl-(l ->4)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(1^3)-0-(β-D-galactopyranosyl)-(l-44)-D- glucopyranose (9), and 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(l->6)-0(β-D-galactopyranosyl)-(l-44)-D-glucopyranose (15) has been described. Their structures have been established by ¹³C NMR spectroscopy.

Original language	English
Pages (from-to)	269-278
Number of pages	10
Journal	Journal of Carbohydrate Chemistry
Volume	10
Issue number	2
DOIs	https://doi.org/10.1080/07328309108543906
State	Published - Jan 1 1991

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Sarkar, A. K., Pawar, S. M., & Matta, K. L. (1991). Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose¹ Journal of Carbohydrate Chemistry, 10(2), 269-278. https://doi.org/10.1080/07328309108543906

Sarkar, Arun K. ; Pawar, Sushama M. ; Matta, Khushi L. / Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose¹ In: Journal of Carbohydrate Chemistry. 1991 ; Vol. 10, No. 2. pp. 269-278.

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title = "Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose1 ",

abstract = "Synthesis of three tetrasaccharides, namely, 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(l-*3)-0-(β-D-galactopyranosyl)- (1 ->4)-β-D-glucopyranose (7), 0-α-L-fucopyranosyl-(l ->4)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(1\textasciicircum{}3)-0-(β-D-galactopyranosyl)-(l-44)-D- glucopyranose (9), and 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(l->6)-0(β-D-galactopyranosyl)-(l-44)-D-glucopyranose (15) has been described. Their structures have been established by 13C NMR spectroscopy.",

author = "Sarkar, \{Arun K.\} and Pawar, \{Sushama M.\} and Matta, \{Khushi L.\}",

year = "1991",

month = jan,

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doi = "10.1080/07328309108543906",

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Sarkar, AK, Pawar, SM & Matta, KL 1991, 'Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose¹ ', Journal of Carbohydrate Chemistry, vol. 10, no. 2, pp. 269-278. https://doi.org/10.1080/07328309108543906

Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose¹ . / Sarkar, Arun K.; Pawar, Sushama M.; Matta, Khushi L.
In: Journal of Carbohydrate Chemistry, Vol. 10, No. 2, 01.01.1991, p. 269-278.

Research output: Contribution to journal › Article › peer-review

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T1 - Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose1

AU - Sarkar, Arun K.

AU - Pawar, Sushama M.

AU - Matta, Khushi L.

PY - 1991/1/1

Y1 - 1991/1/1

N2 - Synthesis of three tetrasaccharides, namely, 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(l-*3)-0-(β-D-galactopyranosyl)- (1 ->4)-β-D-glucopyranose (7), 0-α-L-fucopyranosyl-(l ->4)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(1^3)-0-(β-D-galactopyranosyl)-(l-44)-D- glucopyranose (9), and 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(l->6)-0(β-D-galactopyranosyl)-(l-44)-D-glucopyranose (15) has been described. Their structures have been established by 13C NMR spectroscopy.

AB - Synthesis of three tetrasaccharides, namely, 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(l-*3)-0-(β-D-galactopyranosyl)- (1 ->4)-β-D-glucopyranose (7), 0-α-L-fucopyranosyl-(l ->4)-0-(2-acetamido-2-deoxy-P-D-glucopyranosyl)-(1^3)-0-(β-D-galactopyranosyl)-(l-44)-D- glucopyranose (9), and 0-α-L-fucopyranosyl-(l—»3)-0-(2-acetamido-2-deoxy-β-D-glucopyranosyl)-(l->6)-0(β-D-galactopyranosyl)-(l-44)-D-glucopyranose (15) has been described. Their structures have been established by 13C NMR spectroscopy.

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DO - 10.1080/07328309108543906

M3 - Article

AN - SCOPUS:84956385022

SN - 0732-8303

VL - 10

SP - 269

EP - 278

JO - Journal of Carbohydrate Chemistry

JF - Journal of Carbohydrate Chemistry

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ER -

Sarkar AK, Pawar SM, Matta KL. Synthesis of two isomeric tetrasaccharides 0-α-l-fucopyranosyl-(1—>3) and (l->4)-0-(2-acetamido-2-deoxy-β-d-glucopyranosyl)-(l—>3)-0-(p-d-galactopyranosyl)-(l—»4)-d- glucopyranose and a related tetrasaccharide o-α-l-fucopyranosyl-(l->3)-0-(2-acetamido-2-deoxy-β-d- glucopyranosyl-(l—>6)-0-(β-d-galactopyranosyl)-(l—>4)-d-glucopyranose¹ Journal of Carbohydrate Chemistry. 1991 Jan 1;10(2):269-278. doi: 10.1080/07328309108543906

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