Synthesis of oligosaccharides containing β-d-Gal-(1→3)-O-(6-O-sulfo-β-d-GlcNAc) as a terminal unit

Bao Guo Huang; Rakesh K. Jain; Walter A. Tabaczynski; James L. Alderfer; Khushi L. Matta

doi:10.1016/S0008-6215(98)00166-9

Synthesis of oligosaccharides containing β-d-Gal-(1→3)-O-(6-O-sulfo-β-d-GlcNAc) as a terminal unit

Bao Guo Huang
, Rakesh K. Jain
, Walter A. Tabaczynski
, James L. Alderfer
, Khushi L. Matta

Department of Chemical and Biological Engineering

Roswell Park Cancer Institute
Occidental Petroleum
Inc.

Research output: Contribution to journal › Article › peer-review

2 Scopus citations

Abstract

The chemical synthesis of β-D-Gal-(1→3)-6-O-SO₃Na-β-D-GlcNAc-(1→6)-α-D-Man-O-C₆H₄NO₂ (1) and β-D-Gal-(1→3)-6-O-SO₃Na-β-D-GlcNAc-(1→2)-α-D-Man-OMe (2) is reported using a key glycosyl donor, phenyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1→3)-4,6-di-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside (3). Copyright (C) 1998 Elsevier Science Ltd.

Original language	English
Pages (from-to)	165-169
Number of pages	5
Journal	Carbohydrate Research
Volume	311
Issue number	3
DOIs	https://doi.org/10.1016/S0008-6215(98)00166-9
State	Published - Sep 1998

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@article{5fd82e5a1c684fd89d156c6b2f9d6cc2,

title = "Synthesis of oligosaccharides containing β-d-Gal-(1→3)-O-(6-O-sulfo-β-d-GlcNAc) as a terminal unit",

abstract = "The chemical synthesis of β-D-Gal-(1→3)-6-O-SO3Na-β-D-GlcNAc-(1→6)-α-D-Man-O-C6H4NO2 (1) and β-D-Gal-(1→3)-6-O-SO3Na-β-D-GlcNAc-(1→2)-α-D-Man-OMe (2) is reported using a key glycosyl donor, phenyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1→3)-4,6-di-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside (3). Copyright (C) 1998 Elsevier Science Ltd.",

author = "Huang, \{Bao Guo\} and Jain, \{Rakesh K.\} and Tabaczynski, \{Walter A.\} and Alderfer, \{James L.\} and Matta, \{Khushi L.\}",

year = "1998",

month = sep,

doi = "10.1016/S0008-6215(98)00166-9",

language = "English",

volume = "311",

pages = "165--169",

journal = "Carbohydrate Research",

issn = "0008-6215",

publisher = "Elsevier Ltd",

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T1 - Synthesis of oligosaccharides containing β-d-Gal-(1→3)-O-(6-O-sulfo-β-d-GlcNAc) as a terminal unit

AU - Huang, Bao Guo

AU - Jain, Rakesh K.

AU - Tabaczynski, Walter A.

AU - Alderfer, James L.

AU - Matta, Khushi L.

PY - 1998/9

Y1 - 1998/9

N2 - The chemical synthesis of β-D-Gal-(1→3)-6-O-SO3Na-β-D-GlcNAc-(1→6)-α-D-Man-O-C6H4NO2 (1) and β-D-Gal-(1→3)-6-O-SO3Na-β-D-GlcNAc-(1→2)-α-D-Man-OMe (2) is reported using a key glycosyl donor, phenyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1→3)-4,6-di-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside (3). Copyright (C) 1998 Elsevier Science Ltd.

AB - The chemical synthesis of β-D-Gal-(1→3)-6-O-SO3Na-β-D-GlcNAc-(1→6)-α-D-Man-O-C6H4NO2 (1) and β-D-Gal-(1→3)-6-O-SO3Na-β-D-GlcNAc-(1→2)-α-D-Man-OMe (2) is reported using a key glycosyl donor, phenyl O-(2,3,4,6-tetra-O-acetyl-β-D-galactopyranosyl)-(1→3)-4,6-di-O-chloroacetyl-2-deoxy-2-phthalimido-1-thio-β-D-glucopyranoside (3). Copyright (C) 1998 Elsevier Science Ltd.

UR - https://www.scopus.com/pages/publications/0031760806

U2 - 10.1016/S0008-6215(98)00166-9

DO - 10.1016/S0008-6215(98)00166-9

M3 - Article

C2 - 9825519

AN - SCOPUS:0031760806

SN - 0008-6215

VL - 311

SP - 165

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JO - Carbohydrate Research

JF - Carbohydrate Research

IS - 3

ER -

Synthesis of oligosaccharides containing β-d-Gal-(1→3)-O-(6-O-sulfo-β-d-GlcNAc) as a terminal unit

Abstract

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